{
 "schema": 1,
 "_what": "Neutral database of published independent laboratory results on peptide products, failures included. Schema and provenance rules live in _ops/lab_db.py; this file is the data. Part 1 of roadmap P3-3 defines the structure only: rows are added in later parts, each from a published report.",
 "_naming": "Settled 2026-10-01. A party may be named when someone can vouch for where the vial came from: ONE source is enough if that source obtained the sample itself (a laboratory's own market survey, a regulator's seizure, a journal that bought and tested the product), and TWO INDEPENDENT sources are required when a buyer submitted the sample, which is most grey-market reports. The name on a submitted report is self-declared — the laboratory verifies the contents, never the chain of custody — so naming on one such report would republish an unverified claim about origin and make a mislabelled vial a cheap way to attack a competitor through us. Every source declares `sampling`, required and never defaulted. Enforced in _ops/lab_db.py, gated by check.py:lab_db_provenance, 22-case selftest.",
 "_refuses": [
  "price",
  "purchase links",
  "seller names while party_names_allowed is false",
  "any aggregate score per party"
 ],
 "updated": "2026-10-01",
 "rows": [
  {
   "compound": "semaglutide",
   "party": "PARTY-01",
   "party_name": "Biotech Peptides",
   "party_kind": "illegal-online-pharmacy",
   "batch": "",
   "report_id": "PMID 39509151",
   "tested": "2023-08/2024-03",
   "tested_note": "The research letter on this study states that test purchases and analytical testing were performed from August 2023 to March 2024; neither paper gives a date for any individual test.",
   "samples": 1,
   "sources": [
    {
     "kind": "journal",
     "originator": "Ashraf et al. study team, University of Pécs",
     "sampling": "source-obtained",
     "pmid": "39509151",
     "citation": "Ashraf AR et al. Multifactor Quality and Safety Analysis of Semaglutide Products Sold by Online Sellers Without a Prescription. J Med Internet Res 2024;26:e65440. The study team made the test purchases itself."
    },
    {
     "kind": "journal",
     "originator": "Ashraf et al. study team, University of Pécs",
     "sampling": "source-obtained",
     "pmid": "39093567",
     "citation": "Ashraf AR et al. Safety and Risk Assessment of No-Prescription Online Semaglutide Purchases. JAMA Netw Open 2024;7(8):e2428280. The same study's earlier letter; the source of the testing window."
    }
   ],
   "added": "2026-10-01",
   "id": "LR-0001",
   "measure": "content",
   "result": 3.86,
   "unit": "mg",
   "verdict": "fail",
   "expected": "3 mg of semaglutide per vial, as labelled",
   "method": "LC-MS",
   "lab": "Mass Spectrometry Core Facility, Szentágothai Research Centre, University of Pécs",
   "note": "Measured 3.86 mg (SD 0.14) against 3 mg on the label: 28.56% more than labelled, which is the paper's own labelling-accuracy figure. The same method read the genuine Ozempic 1 mg pen at +5.05% over its label. A reader dosing by the label would receive more than intended. Named under the sample-control rule: the study team bought this product itself, and the paper reports its results separately from the other products."
  },
  {
   "compound": "semaglutide",
   "party": "PARTY-01",
   "party_name": "Biotech Peptides",
   "party_kind": "illegal-online-pharmacy",
   "batch": "",
   "report_id": "PMID 39509151",
   "tested": "2023-08/2024-03",
   "tested_note": "The research letter on this study states that test purchases and analytical testing were performed from August 2023 to March 2024; neither paper gives a date for any individual test.",
   "samples": 1,
   "sources": [
    {
     "kind": "journal",
     "originator": "Ashraf et al. study team, University of Pécs",
     "sampling": "source-obtained",
     "pmid": "39509151",
     "citation": "Ashraf AR et al. Multifactor Quality and Safety Analysis of Semaglutide Products Sold by Online Sellers Without a Prescription. J Med Internet Res 2024;26:e65440. The study team made the test purchases itself."
    },
    {
     "kind": "journal",
     "originator": "Ashraf et al. study team, University of Pécs",
     "sampling": "source-obtained",
     "pmid": "39093567",
     "citation": "Ashraf AR et al. Safety and Risk Assessment of No-Prescription Online Semaglutide Purchases. JAMA Netw Open 2024;7(8):e2428280. The same study's earlier letter; the source of the testing window."
    }
   ],
   "added": "2026-10-01",
   "id": "LR-0002",
   "measure": "purity",
   "result": 7.7,
   "unit": "%",
   "verdict": "inconclusive",
   "expected": "99%, as stated on the product label or website",
   "method": "LC-MS",
   "lab": "Mass Spectrometry Core Facility, Szentágothai Research Centre, University of Pécs",
   "note": "The paper's purity is semaglutide as a share of the whole powder in the vial (3.86 mg of 50.1 mg), not the chromatographic peptide purity a research-grade '99%' claim usually means; the paper found no peptide-like impurities. So the vial is mostly undeclared non-peptide material, and the two percentages measure different things. The measurement stands; the comparison is not like-for-like. Named under the sample-control rule: the study team bought this product itself, and the paper reports its results separately from the other products."
  },
  {
   "compound": "semaglutide",
   "party": "PARTY-01",
   "party_name": "Biotech Peptides",
   "party_kind": "illegal-online-pharmacy",
   "batch": "",
   "report_id": "PMID 39509151",
   "tested": "2023-08/2024-03",
   "tested_note": "The research letter on this study states that test purchases and analytical testing were performed from August 2023 to March 2024; neither paper gives a date for any individual test.",
   "samples": 1,
   "sources": [
    {
     "kind": "journal",
     "originator": "Ashraf et al. study team, University of Pécs",
     "sampling": "source-obtained",
     "pmid": "39509151",
     "citation": "Ashraf AR et al. Multifactor Quality and Safety Analysis of Semaglutide Products Sold by Online Sellers Without a Prescription. J Med Internet Res 2024;26:e65440. The study team made the test purchases itself."
    },
    {
     "kind": "journal",
     "originator": "Ashraf et al. study team, University of Pécs",
     "sampling": "source-obtained",
     "pmid": "39093567",
     "citation": "Ashraf AR et al. Safety and Risk Assessment of No-Prescription Online Semaglutide Purchases. JAMA Netw Open 2024;7(8):e2428280. The same study's earlier letter; the source of the testing window."
    }
   ],
   "added": "2026-10-01",
   "id": "LR-0003",
   "measure": "sterility",
   "result": "no viable microorganisms",
   "unit": "",
   "verdict": "pass",
   "expected": "sterile, per Ph. Eur. 2.6.1 and USP <71>",
   "method": "USP-71",
   "lab": "PharmaValid Ltd microbiology laboratory, Budapest (ISO 14644-1 certified)",
   "note": "Tested by what the paper calls a direct injection technique, under both pharmacopoeias. The paper reports the lyophilised powder free of viable microorganisms at the time of testing; it does not test the vial after reconstitution or storage. Named under the sample-control rule: the study team bought this product itself, and the paper reports its results separately from the other products."
  },
  {
   "compound": "semaglutide",
   "party": "PARTY-01",
   "party_name": "Biotech Peptides",
   "party_kind": "illegal-online-pharmacy",
   "batch": "",
   "report_id": "PMID 39509151",
   "tested": "2023-08/2024-03",
   "tested_note": "The research letter on this study states that test purchases and analytical testing were performed from August 2023 to March 2024; neither paper gives a date for any individual test.",
   "samples": 1,
   "sources": [
    {
     "kind": "journal",
     "originator": "Ashraf et al. study team, University of Pécs",
     "sampling": "source-obtained",
     "pmid": "39509151",
     "citation": "Ashraf AR et al. Multifactor Quality and Safety Analysis of Semaglutide Products Sold by Online Sellers Without a Prescription. J Med Internet Res 2024;26:e65440. The study team made the test purchases itself."
    },
    {
     "kind": "journal",
     "originator": "Ashraf et al. study team, University of Pécs",
     "sampling": "source-obtained",
     "pmid": "39093567",
     "citation": "Ashraf AR et al. Safety and Risk Assessment of No-Prescription Online Semaglutide Purchases. JAMA Netw Open 2024;7(8):e2428280. The same study's earlier letter; the source of the testing window."
    }
   ],
   "added": "2026-10-01",
   "id": "LR-0004",
   "measure": "endotoxin",
   "result": "<2.1645",
   "unit": "EU/mg",
   "verdict": "inconclusive",
   "expected": "no acceptance limit is stated in the source for this product",
   "method": "LAL",
   "lab": "PharmaValid Ltd microbiology laboratory, Budapest (ISO 14644-1 certified)",
   "note": "Reported as below 2.1645 EU/mg by kinetic turbidimetric assay (Ph. Eur. 2.6.14, USP <85>) — an upper bound, not a measured level, although the paper's abstract describes endotoxin as detected in all samples. No limit is stated, so no pass or fail is given here. Named under the sample-control rule: the study team bought this product itself, and the paper reports its results separately from the other products."
  },
  {
   "compound": "semaglutide",
   "party": "PARTY-02",
   "party_name": "SemaSpace",
   "party_kind": "illegal-online-pharmacy",
   "batch": "",
   "report_id": "PMID 39509151",
   "tested": "2023-08/2024-03",
   "tested_note": "The research letter on this study states that test purchases and analytical testing were performed from August 2023 to March 2024; neither paper gives a date for any individual test.",
   "samples": 1,
   "sources": [
    {
     "kind": "journal",
     "originator": "Ashraf et al. study team, University of Pécs",
     "sampling": "source-obtained",
     "pmid": "39509151",
     "citation": "Ashraf AR et al. Multifactor Quality and Safety Analysis of Semaglutide Products Sold by Online Sellers Without a Prescription. J Med Internet Res 2024;26:e65440. The study team made the test purchases itself."
    },
    {
     "kind": "journal",
     "originator": "Ashraf et al. study team, University of Pécs",
     "sampling": "source-obtained",
     "pmid": "39093567",
     "citation": "Ashraf AR et al. Safety and Risk Assessment of No-Prescription Online Semaglutide Purchases. JAMA Netw Open 2024;7(8):e2428280. The same study's earlier letter; the source of the testing window."
    }
   ],
   "added": "2026-10-01",
   "id": "LR-0005",
   "measure": "content",
   "result": 2.77,
   "unit": "mg",
   "verdict": "fail",
   "expected": "2 mg of semaglutide per vial, as labelled",
   "method": "LC-MS",
   "lab": "Mass Spectrometry Core Facility, Szentágothai Research Centre, University of Pécs",
   "note": "Measured 2.77 mg (SD 0.12) against 2 mg on the label: 38.69% more than labelled, which is the paper's own labelling-accuracy figure. The same method read the genuine Ozempic 1 mg pen at +5.05% over its label. A reader dosing by the label would receive more than intended. Named under the sample-control rule: the study team bought this product itself, and the paper reports its results separately from the other products."
  },
  {
   "compound": "semaglutide",
   "party": "PARTY-02",
   "party_name": "SemaSpace",
   "party_kind": "illegal-online-pharmacy",
   "batch": "",
   "report_id": "PMID 39509151",
   "tested": "2023-08/2024-03",
   "tested_note": "The research letter on this study states that test purchases and analytical testing were performed from August 2023 to March 2024; neither paper gives a date for any individual test.",
   "samples": 1,
   "sources": [
    {
     "kind": "journal",
     "originator": "Ashraf et al. study team, University of Pécs",
     "sampling": "source-obtained",
     "pmid": "39509151",
     "citation": "Ashraf AR et al. Multifactor Quality and Safety Analysis of Semaglutide Products Sold by Online Sellers Without a Prescription. J Med Internet Res 2024;26:e65440. The study team made the test purchases itself."
    },
    {
     "kind": "journal",
     "originator": "Ashraf et al. study team, University of Pécs",
     "sampling": "source-obtained",
     "pmid": "39093567",
     "citation": "Ashraf AR et al. Safety and Risk Assessment of No-Prescription Online Semaglutide Purchases. JAMA Netw Open 2024;7(8):e2428280. The same study's earlier letter; the source of the testing window."
    }
   ],
   "added": "2026-10-01",
   "id": "LR-0006",
   "measure": "purity",
   "result": 14.37,
   "unit": "%",
   "verdict": "inconclusive",
   "expected": "99%, as stated on the product label or website",
   "method": "LC-MS",
   "lab": "Mass Spectrometry Core Facility, Szentágothai Research Centre, University of Pécs",
   "note": "The paper's purity is semaglutide as a share of the whole powder in the vial (2.77 mg of 19.3 mg), not the chromatographic peptide purity a research-grade '99%' claim usually means; the paper found no peptide-like impurities. So the vial is mostly undeclared non-peptide material, and the two percentages measure different things. The measurement stands; the comparison is not like-for-like. Named under the sample-control rule: the study team bought this product itself, and the paper reports its results separately from the other products."
  },
  {
   "compound": "semaglutide",
   "party": "PARTY-02",
   "party_name": "SemaSpace",
   "party_kind": "illegal-online-pharmacy",
   "batch": "",
   "report_id": "PMID 39509151",
   "tested": "2023-08/2024-03",
   "tested_note": "The research letter on this study states that test purchases and analytical testing were performed from August 2023 to March 2024; neither paper gives a date for any individual test.",
   "samples": 1,
   "sources": [
    {
     "kind": "journal",
     "originator": "Ashraf et al. study team, University of Pécs",
     "sampling": "source-obtained",
     "pmid": "39509151",
     "citation": "Ashraf AR et al. Multifactor Quality and Safety Analysis of Semaglutide Products Sold by Online Sellers Without a Prescription. J Med Internet Res 2024;26:e65440. The study team made the test purchases itself."
    },
    {
     "kind": "journal",
     "originator": "Ashraf et al. study team, University of Pécs",
     "sampling": "source-obtained",
     "pmid": "39093567",
     "citation": "Ashraf AR et al. Safety and Risk Assessment of No-Prescription Online Semaglutide Purchases. JAMA Netw Open 2024;7(8):e2428280. The same study's earlier letter; the source of the testing window."
    }
   ],
   "added": "2026-10-01",
   "id": "LR-0007",
   "measure": "sterility",
   "result": "no viable microorganisms",
   "unit": "",
   "verdict": "pass",
   "expected": "sterile, per Ph. Eur. 2.6.1 and USP <71>",
   "method": "USP-71",
   "lab": "PharmaValid Ltd microbiology laboratory, Budapest (ISO 14644-1 certified)",
   "note": "Tested by what the paper calls a direct injection technique, under both pharmacopoeias. The paper reports the lyophilised powder free of viable microorganisms at the time of testing; it does not test the vial after reconstitution or storage. Named under the sample-control rule: the study team bought this product itself, and the paper reports its results separately from the other products."
  },
  {
   "compound": "semaglutide",
   "party": "PARTY-02",
   "party_name": "SemaSpace",
   "party_kind": "illegal-online-pharmacy",
   "batch": "",
   "report_id": "PMID 39509151",
   "tested": "2023-08/2024-03",
   "tested_note": "The research letter on this study states that test purchases and analytical testing were performed from August 2023 to March 2024; neither paper gives a date for any individual test.",
   "samples": 1,
   "sources": [
    {
     "kind": "journal",
     "originator": "Ashraf et al. study team, University of Pécs",
     "sampling": "source-obtained",
     "pmid": "39509151",
     "citation": "Ashraf AR et al. Multifactor Quality and Safety Analysis of Semaglutide Products Sold by Online Sellers Without a Prescription. J Med Internet Res 2024;26:e65440. The study team made the test purchases itself."
    },
    {
     "kind": "journal",
     "originator": "Ashraf et al. study team, University of Pécs",
     "sampling": "source-obtained",
     "pmid": "39093567",
     "citation": "Ashraf AR et al. Safety and Risk Assessment of No-Prescription Online Semaglutide Purchases. JAMA Netw Open 2024;7(8):e2428280. The same study's earlier letter; the source of the testing window."
    }
   ],
   "added": "2026-10-01",
   "id": "LR-0008",
   "measure": "endotoxin",
   "result": "8.9511",
   "unit": "EU/mg",
   "verdict": "inconclusive",
   "expected": "no acceptance limit is stated in the source for this product",
   "method": "LAL",
   "lab": "PharmaValid Ltd microbiology laboratory, Budapest (ISO 14644-1 certified)",
   "note": "Endotoxin measured at 8.9511 EU/mg by kinetic turbidimetric assay (Ph. Eur. 2.6.14, USP <85>), the highest of the three; the paper says it indicates potential environmental contamination during production. No limit is stated, so no pass or fail is given here. Named under the sample-control rule: the study team bought this product itself, and the paper reports its results separately from the other products."
  },
  {
   "compound": "semaglutide",
   "party": "PARTY-03",
   "party_name": "USChemLabs",
   "party_kind": "illegal-online-pharmacy",
   "batch": "",
   "report_id": "PMID 39509151",
   "tested": "2023-08/2024-03",
   "tested_note": "The research letter on this study states that test purchases and analytical testing were performed from August 2023 to March 2024; neither paper gives a date for any individual test.",
   "samples": 1,
   "sources": [
    {
     "kind": "journal",
     "originator": "Ashraf et al. study team, University of Pécs",
     "sampling": "source-obtained",
     "pmid": "39509151",
     "citation": "Ashraf AR et al. Multifactor Quality and Safety Analysis of Semaglutide Products Sold by Online Sellers Without a Prescription. J Med Internet Res 2024;26:e65440. The study team made the test purchases itself."
    },
    {
     "kind": "journal",
     "originator": "Ashraf et al. study team, University of Pécs",
     "sampling": "source-obtained",
     "pmid": "39093567",
     "citation": "Ashraf AR et al. Safety and Risk Assessment of No-Prescription Online Semaglutide Purchases. JAMA Netw Open 2024;7(8):e2428280. The same study's earlier letter; the source of the testing window."
    }
   ],
   "added": "2026-10-01",
   "id": "LR-0009",
   "measure": "content",
   "result": 1.34,
   "unit": "mg",
   "verdict": "fail",
   "expected": "1 mg of semaglutide per vial, as labelled",
   "method": "LC-MS",
   "lab": "Mass Spectrometry Core Facility, Szentágothai Research Centre, University of Pécs",
   "note": "Measured 1.34 mg (SD 0.07) against 1 mg on the label: 33.58% more than labelled, which is the paper's own labelling-accuracy figure. The same method read the genuine Ozempic 1 mg pen at +5.05% over its label. A reader dosing by the label would receive more than intended. Named under the sample-control rule: the study team bought this product itself, and the paper reports its results separately from the other products."
  },
  {
   "compound": "semaglutide",
   "party": "PARTY-03",
   "party_name": "USChemLabs",
   "party_kind": "illegal-online-pharmacy",
   "batch": "",
   "report_id": "PMID 39509151",
   "tested": "2023-08/2024-03",
   "tested_note": "The research letter on this study states that test purchases and analytical testing were performed from August 2023 to March 2024; neither paper gives a date for any individual test.",
   "samples": 1,
   "sources": [
    {
     "kind": "journal",
     "originator": "Ashraf et al. study team, University of Pécs",
     "sampling": "source-obtained",
     "pmid": "39509151",
     "citation": "Ashraf AR et al. Multifactor Quality and Safety Analysis of Semaglutide Products Sold by Online Sellers Without a Prescription. J Med Internet Res 2024;26:e65440. The study team made the test purchases itself."
    },
    {
     "kind": "journal",
     "originator": "Ashraf et al. study team, University of Pécs",
     "sampling": "source-obtained",
     "pmid": "39093567",
     "citation": "Ashraf AR et al. Safety and Risk Assessment of No-Prescription Online Semaglutide Purchases. JAMA Netw Open 2024;7(8):e2428280. The same study's earlier letter; the source of the testing window."
    }
   ],
   "added": "2026-10-01",
   "id": "LR-0010",
   "measure": "purity",
   "result": 8.97,
   "unit": "%",
   "verdict": "inconclusive",
   "expected": "99%, as stated on the product label or website",
   "method": "LC-MS",
   "lab": "Mass Spectrometry Core Facility, Szentágothai Research Centre, University of Pécs",
   "note": "The paper's purity is semaglutide as a share of the whole powder in the vial (1.34 mg of 14.9 mg), not the chromatographic peptide purity a research-grade '99%' claim usually means; the paper found no peptide-like impurities. So the vial is mostly undeclared non-peptide material, and the two percentages measure different things. The measurement stands; the comparison is not like-for-like. Named under the sample-control rule: the study team bought this product itself, and the paper reports its results separately from the other products."
  },
  {
   "compound": "semaglutide",
   "party": "PARTY-03",
   "party_name": "USChemLabs",
   "party_kind": "illegal-online-pharmacy",
   "batch": "",
   "report_id": "PMID 39509151",
   "tested": "2023-08/2024-03",
   "tested_note": "The research letter on this study states that test purchases and analytical testing were performed from August 2023 to March 2024; neither paper gives a date for any individual test.",
   "samples": 1,
   "sources": [
    {
     "kind": "journal",
     "originator": "Ashraf et al. study team, University of Pécs",
     "sampling": "source-obtained",
     "pmid": "39509151",
     "citation": "Ashraf AR et al. Multifactor Quality and Safety Analysis of Semaglutide Products Sold by Online Sellers Without a Prescription. J Med Internet Res 2024;26:e65440. The study team made the test purchases itself."
    },
    {
     "kind": "journal",
     "originator": "Ashraf et al. study team, University of Pécs",
     "sampling": "source-obtained",
     "pmid": "39093567",
     "citation": "Ashraf AR et al. Safety and Risk Assessment of No-Prescription Online Semaglutide Purchases. JAMA Netw Open 2024;7(8):e2428280. The same study's earlier letter; the source of the testing window."
    }
   ],
   "added": "2026-10-01",
   "id": "LR-0011",
   "measure": "sterility",
   "result": "no viable microorganisms",
   "unit": "",
   "verdict": "pass",
   "expected": "sterile, per Ph. Eur. 2.6.1 and USP <71>",
   "method": "USP-71",
   "lab": "PharmaValid Ltd microbiology laboratory, Budapest (ISO 14644-1 certified)",
   "note": "Tested by what the paper calls a direct injection technique, under both pharmacopoeias. The paper reports the lyophilised powder free of viable microorganisms at the time of testing; it does not test the vial after reconstitution or storage. Named under the sample-control rule: the study team bought this product itself, and the paper reports its results separately from the other products."
  },
  {
   "compound": "semaglutide",
   "party": "PARTY-03",
   "party_name": "USChemLabs",
   "party_kind": "illegal-online-pharmacy",
   "batch": "",
   "report_id": "PMID 39509151",
   "tested": "2023-08/2024-03",
   "tested_note": "The research letter on this study states that test purchases and analytical testing were performed from August 2023 to March 2024; neither paper gives a date for any individual test.",
   "samples": 1,
   "sources": [
    {
     "kind": "journal",
     "originator": "Ashraf et al. study team, University of Pécs",
     "sampling": "source-obtained",
     "pmid": "39509151",
     "citation": "Ashraf AR et al. Multifactor Quality and Safety Analysis of Semaglutide Products Sold by Online Sellers Without a Prescription. J Med Internet Res 2024;26:e65440. The study team made the test purchases itself."
    },
    {
     "kind": "journal",
     "originator": "Ashraf et al. study team, University of Pécs",
     "sampling": "source-obtained",
     "pmid": "39093567",
     "citation": "Ashraf AR et al. Safety and Risk Assessment of No-Prescription Online Semaglutide Purchases. JAMA Netw Open 2024;7(8):e2428280. The same study's earlier letter; the source of the testing window."
    }
   ],
   "added": "2026-10-01",
   "id": "LR-0012",
   "measure": "endotoxin",
   "result": "<2.8658",
   "unit": "EU/mg",
   "verdict": "inconclusive",
   "expected": "no acceptance limit is stated in the source for this product",
   "method": "LAL",
   "lab": "PharmaValid Ltd microbiology laboratory, Budapest (ISO 14644-1 certified)",
   "note": "Reported as below 2.8658 EU/mg by kinetic turbidimetric assay (Ph. Eur. 2.6.14, USP <85>) — an upper bound, not a measured level, although the paper's abstract describes endotoxin as detected in all samples. No limit is stated, so no pass or fail is given here. Named under the sample-control rule: the study team bought this product itself, and the paper reports its results separately from the other products."
  }
 ],
 "party_naming": "sample-control"
}